Thursday, December 9, 2010

Reaction #5 - How to make carbonic acid

Carbonic acid is a weak acid, but if you want to make it, here's how:
Materials:
  • Vinegar / calcium chloride powder (vinegar - please follow normal steps and "A" steps, calcium chloride - please follow normal steps and "B" steps)
  • Sodium bicarbonate
  • Water
  • 25ml graduating cylinder
  • 1000ml (1 litre) beaker
  • Conical flask with hole at the side that connects to a glass pipette
  • Stopper
Step 1: Place the 25ml graduating cylinder into the 1000ml beaker.
Step 2: Pour the sodium bicarbonate into the conical flask.
Step 3: Pour water into the graduating cylinder.
Step 4: Put the glass pipette into the graduating cylinder.
Step 5A: Pour the vinegar (a bit will do) into the conical flask and stopper it off.
Step 5B: Add the calcium chloride into the conical flask and then add 10 ml of water (stopper it off immediately).
Step 6: Wait till no more gas bubbles come out of the pipette.
Step 7: Obtain the product (it's in the graduating cylinder)
Here're the chemical equations of this process:
For A:
Sodium bicarbonate + Vinegar (Acetic / ethanoic acid) Sodium acetate / ethanoate + Water + Carbon dioxide
NaHCO3 + CH3COOH CH3COONa + H2O + CO2
For B:
Sodium bicarbonate + Calcium chloride Sodium chloride + Calcium carbonate + Water + Carbon dioxide
2NaHCO3 + CaCl2 2NaCl + CaCO3 + H2O + CO2
(This actually goes in a multi-step process but I'm just simplifying it here.)
In both steps, the carbon dioxide dissolves into the water in the graduating cylinder to form carbonic acid:
Carbon dioxide + Water → Carbonic acid
CO2 + H2O H2CO3
Improvements: Add crushed ice and water to the beaker containing the graduating cylinder (increases yield because gases dissolve better in colder water).
 
Good luck! 加油!

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